O-methoxybenzaldehyde

Description:

Ex salicylaldehyde per methylationem reactionem cum sulphate dimethyl.Misce 3kg hydroxidi sodii in solutionem aqueam 30%, adde 12.2kg de salicylaldehyde et 80L aquae excitando, et calori ad ferventem.Tarde 12.9kg de sulphate dimethyli adde, solutionem reactionis refluxisse pro 3h circiter additis, pergere ad refluentem pro 2-3h sequenti Chemicalbook...


Product Detail

Product Tags

Formulae structurales

19

Sinica nomen:o-methoxybenzaldehyde

Aliud nomen;o-methoxybenzaldehyde;2-methoxybenzaldehyde;2-anisaldehyde;o-anisaldehyde;o-methoxybenzaldehyde;salicaldehyde yl aether;o-anisaldehyde;salicylaldehyde yl aether

Formulae hypotheticae:C8H8O2

Pondus hypotheticum:136.15

Numerus Systema

CAS Number:135-02-4

EINECS:205-171-7

codicem HS;29124900

Technical Parameters

Aspectus: hyalina prismatica crystallo

Puritas: ≥98.0%

Punctum liquescens: 39°C

Fervens punctum: 238°C, 70-75°C/0.2kPa

Densitas relativa: 1.1326 (20/4°C)

Index refractivus: 1.5597

Micare punctum: 117°C

Solubilitas: solutum in alcohole, aethere, benzene, in aqua solutum

Productio Methodo

Ex salicylaldehyde per methylationem reactionem cum sulphate dimethyl.Misce 3kg hydroxidi sodii in solutionem aqueam 30%, adde 12.2kg de salicylaldehyde et 80L aquae excitando, et calori ad ferventem.Tarde 12.9kg de sulphate dimethyli adde, solutionem reactionis refluxisse per 3h circiter additis, pergere ad refluentem pro 2-3h sequenti Chemicalbook, lavacrum oleum refrigerare, solutionem sodium sodium 5% lava, et postea cum aqua ad pH 8 lava. adde carbonas anhydrous potassae exsiccatae.Post eliquationem desiccant, distillationem pressionem reductam colligens destillationem ad 120°C (2.0kPa), quod est o-methoxybenzaldehyde.Reactio methylatio etiam exerceri potest in toluene solvendo, cum fructu 60%.

Propositum

Methoxybenzaldehyde est media synthesis organica, quae adhibetur in productione aromatum et medicamentorum.O-methoxybenformaldehyde productio adhiberi potest.O-Methoxybenzaldehyde adhiberi potest ad medicamento adrenergicum producendum Chuankening.


  • Previous:
  • Deinde:

  • Epistulam tuam hic scribe et mitte nobis